Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Hydrochloric Acid → Phenylmaleic anhydride
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Hydrochloric Acid | HCID 313 | — |
| 반응물 | Aniline | HCID 6115 | — |
| 반응물 | Maleic Anhydride | HCID 7923 | — |
| 용매 | Acetonitrile | HCID 6342 | — |
| 생성물 | Phenylmaleic anhydride | HCID 99174 | 29.2% |
반응 단계
Following the general procedure of Example I, 150 mmols of maleic anhydride were reacted with 25 mmols of distilled aniline in 60 mL of acetonitrile and in the presence of 38 mmols of concentrated HCl and 2.5 mmols of cuprous oxide. The process resulted in a 29.2% yield of 3-phenylmaleic anhydride.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04604243 |
| 출처 데이터셋 | uspto-grants-1986_08 |
| ORD ID | ord-af992a265b0f4d518bc1668be33d9b29 |
| 출처 메모 | uspto-grants-1986_08 |