Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Formic Acid → 3-(3,4-Dimethoxyphenyl)propionic acid
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Formic Acid | HCID 284 | — |
| 반응물 | Veratraldehyde | HCID 8419 | — |
| 반응물 | 2,2-Dimethyl-1,3-dioxane-4,6-dione | HCID 16249 | — |
| 용매 | Triethylamine | HCID 8471 | — |
| 생성물 | 3-(3,4-Dimethoxyphenyl)propionic acid | HCID 75019 | — |
반응 단계
7.2 g (0.05 mol) of Meldrum's acid and 8.3 g (0.05 mol) of veratraldehyde were weighed to 40 ml of the mixture of formic acid and triethylamine recovered by distillation in Example 3. The reaction was carried out and the final product was separated as described in Example 3. The volume of the mixture of formic acid and triethylamine recovered amounted to 28 ml.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US05414108 |
| 출처 데이터셋 | uspto-grants-1995_05 |
| ORD ID | ord-898655059bc74a8987c73528375cf1ae |
| 출처 메모 | uspto-grants-1995_05 |