Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Formic Acid → 3,4,5-Trimethoxyhydrocinnamic acid
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Formic Acid | HCID 284 | — |
| 반응물 | 2,2-Dimethyl-5-(3,4,5-trimethoxybenzylidene)-1,3-dioxane-4,6-dione | HCID 370323 | — |
| 용매 | Triethylamine | HCID 8471 | — |
| 생성물 | 3,4,5-Trimethoxyhydrocinnamic acid | HCID 64860 | — |
반응 단계
16.1 g (0.05 mol) of 5-(3,4,5-trimethoxyphenylmethylene)-2,2-dimethyl-1,3-dioxane-4,6-dione (m.p.: 159°-160° C.) were added to 50 ml of the mixture of formic acid and triethylamine prepared as described in Example 1, then the procedure described in Example 2 was followed.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US05414108 |
| 출처 데이터셋 | uspto-grants-1995_05 |
| ORD ID | ord-9a4790b671d943c98b12419b5845869e |
| 출처 메모 | uspto-grants-1995_05 |