Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Potassium Carbonate → 1-(2-Hydrazinylethyl)pyrrolidine
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Potassium Carbonate | HCID 11430 | — |
| 반응물 | Sodium Hydroxide | HCID 14798 | — |
| 반응물 | Hydrazine hydrate (1:1) | HCID 24654 | — |
| 반응물 | 1-(2-Chloroethyl)pyrrolidine hydrochloride | HCID 81668 | — |
| 용매 | Water | HCID 962 | — |
| 생성물 | 1-(2-Hydrazinylethyl)pyrrolidine | HCID 3031556 | — |
반응 단계
A mixture of 200 g of 85% hydrazine hydrate, 200 ml of water, 170 g of N-chloroethylpyrrolidine hydrochloride, and 70 g of potassium carbonate was boiled under reflux for seven hours. Sodium hydroxide (390 g) was added and the mixture was extracted with ether. The ethereal extract, dried and distilled, yielded the title compound, bp 107°-111° C. (18.5 mm).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04604390 |
| 출처 데이터셋 | uspto-grants-1986_08 |
| ORD ID | ord-16204511989e437e8028f0fb62d2c3b9 |
| 출처 메모 | uspto-grants-1986_08 |