Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Pyridine → Glycidyl benzoate
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Pyridine | HCID 1049 | — |
| 반응물 | Benzoyl chloride | HCID 7412 | — |
| 반응물 | Glycidol | HCID 11164 | — |
| 용매 | Diethyl Ether | HCID 3283 | — |
| 생성물 | Glycidyl benzoate | HCID 25998 | 60% |
반응 단계
A mixture containing 14.8 g (0.2 mole) of glycidol, 150 ml of anhydrous ether, 16 g (0.4 mole) of pyridine and 28 g (0.2 mole) of benzoyl chloride was stirred at room temperature for 2 hours. The mixture was filtered and the ether was evaporated to leave an oil. This oil was distilled to give 21 g (60%) of colorless oil: b.p. 92° C./0.5 mm Hg. The NMR and IR spectra were consistent with the assigned structure.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04604481 |
| 출처 데이터셋 | uspto-grants-1986_08 |
| ORD ID | ord-c63f62e849684cd993425acaf0a156f2 |
| 출처 메모 | uspto-grants-1986_08 |