Potassium Carbonate → HCID 178472279, 화합물

HRID 36452

반응식

HRID 36452 반응식
[CH2:1]([O:3][CH:4]([PH:8](=[O:12])OCC)[O:5][CH2:6][CH3:7])[CH3:2].[CH:13]1([Mg]Cl)[CH2:18][CH2:17][CH2:16][CH2:15][CH2:14]1.C(=O)([O-])[O-].[K+].[K+]>C(OCC)C.O>[CH:13]1([PH:8](=[O:12])[CH:4]([O:3][CH2:1][CH3:2])[O:5][CH2:6][CH3:7])[CH2:18][CH2:17][CH2:16][CH2:15][CH2:14]1

참가 물질

6

반응물 3

HCID 11430Potassium CarbonateHCID 178472284HCID 178472284, 화합물HCID 178478990HCID 178478990, 화합물

생성물 1

HCID 178472279HCID 178472279, 화합물

시약·촉매·용매 2

HCID 962Water용매HCID 3283Diethyl Ether용매

실험 절차

Following a procedure analogous to that of Example 1, but using 9.81 g of ethyl diethoxymethylphosphinate and 50 ml of a 2 molar solution of cyclohexylmagnesium chloride in diethyl ether and adding 20.7 g of potassium carbonate in 25 ml of water to precipitate inorganic salts, cyclohexyl(diethoxymethyl)phosphine oxide is obtained as colourless oil.

후처리

  1. customto precipitate inorganic salts

출처 및 근거

ORD 기록
ord-c3a82320d5ab433b9198f9b8395980f1
출처 데이터셋
uspto-grants-1995_05
특허 번호
US05414133

연결된 노트

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