참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|
| 반응물 | Water | HCID 962 | — |
| 반응물 | Phenylacetone | HCID 7678 | — |
| 반응물 | Sodium Hydroxide | HCID 14798 | — |
| 용매 | Ethanol | HCID 702 | — |
| 생성물 | 1-Phenyl-2-propanol | HCID 94185 | — |
반응 단계
In a 4 liter three-necked flask fitted with a mechanical stirrer and a reflux condenser, were placed 1500 ml of water, 150 g of sodium hydroxide (pellets), 190 ml of ethanol and 180 g of phenylacetone. The mixture was stirred and heated to 80° C., and 150 g of Raney alloy was added very cautiously by small amounts over about 1 hour. During the addition, heating was discontinued and the temperature was maintained at 85°-87° C.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| 특허 번호 | US04605697 |
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| 출처 데이터셋 | uspto-grants-1986_08 |
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| ORD ID | ord-7980c0af962546c2b39c33a7e01dbfdf |
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| 출처 메모 | uspto-grants-1986_08 |
|---|