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Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
HRID 364833생성일: 2026년 10월 27일

Hydrochloric Acid → HCID 178526577, 화합물

https://huagongshe.com/reaction/364833

반응식

참여 물질

역할이름HCID투입량
반응물Hydrochloric AcidHCID 313—
반응물WaterHCID 962—
반응물Carbon DisulfideHCID 6348—
반응물o-NitrobenzohydrazideHCID 3781218—
용매PyridineHCID 1049—
생성물HCID 178526577HCID 178526577—

반응 단계

The reactions of Equation 36 above can be run according to similar procedures described in E. Hoggarth, J. Chem. Soc., 4811 (1952). Thus, in reaction 36a, 2-nitrobenzhydrazide XLVIII is reacted with carbon disulfide in pyridine solvent at 25° to 80° C. for about 4 to 16 hours, followed by addition of water and acidification with hydrochloric acid to form a 2-mercapto-5-(2-nitrophenyl)-1,3,4-oxadiazole of Formula (L). In reaction 36b, L is reacted with sodium hydroxide and methyl iodide in water at 0° to 30° C. for 0.2 to 1 hour to form Xk".

출처 및 근거

DOI10.6084/m9.figshare.5104873.v1
특허 번호US04606755
출처 데이터셋uspto-grants-1986_08
ORD IDord-87d624fc81a841f595958e03c282dd7d
출처 메모uspto-grants-1986_08