Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Hydrochloric Acid → HCID 178526577, 화합물
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Hydrochloric Acid | HCID 313 | — |
| 반응물 | Water | HCID 962 | — |
| 반응물 | Carbon Disulfide | HCID 6348 | — |
| 반응물 | o-Nitrobenzohydrazide | HCID 3781218 | — |
| 용매 | Pyridine | HCID 1049 | — |
| 생성물 | HCID 178526577 | HCID 178526577 | — |
반응 단계
The reactions of Equation 36 above can be run according to similar procedures described in E. Hoggarth, J. Chem. Soc., 4811 (1952). Thus, in reaction 36a, 2-nitrobenzhydrazide XLVIII is reacted with carbon disulfide in pyridine solvent at 25° to 80° C. for about 4 to 16 hours, followed by addition of water and acidification with hydrochloric acid to form a 2-mercapto-5-(2-nitrophenyl)-1,3,4-oxadiazole of Formula (L). In reaction 36b, L is reacted with sodium hydroxide and methyl iodide in water at 0° to 30° C. for 0.2 to 1 hour to form Xk".
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04606755 |
| 출처 데이터셋 | uspto-grants-1986_08 |
| ORD ID | ord-87d624fc81a841f595958e03c282dd7d |
| 출처 메모 | uspto-grants-1986_08 |