Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Potassium Carbonate → 4-Aminocarbonylphenoxyacetic acid methylester
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Potassium Carbonate | HCID 11430 | — |
| 반응물 | Methyl bromoacetate | HCID 60984 | — |
| 반응물 | 4-Hydroxybenzamide | HCID 65052 | — |
| 용매 | Water | HCID 962 | — |
| 용매 | Dimethylformamide | HCID 6228 | — |
| 생성물 | 4-Aminocarbonylphenoxyacetic acid methylester | HCID 8607870 | 63% |
반응 단계
A mixture of p-hydroxybenzamide (3.43 g), methyl bromoacetate (2.37 ml) and K2CO3 (3.45 g) was stirred for 12 hr in 25 ml of DMF. The reaction mixture was diluted with water (150 ml); the solid was filtered, washed with water, and air dried. Crystallization from ethanol gave 3.3 g (63%) of the title compound as white crystals.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US05414132 |
| 출처 데이터셋 | uspto-grants-1995_05 |
| ORD ID | ord-660078129add4fc29c165ea2d40c339c |
| 출처 메모 | uspto-grants-1995_05 |