Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Ammonia → 6-(N-Chloroacetylaminomethyl)-5-hydroxy-4-sulfamoylindane
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Ammonia | HCID 222 | — |
| 반응물 | 6-(N-Chloroacetylaminomethyl)-5-hydroxy-4-chlorosulfonylindane | HCID 21296931 | — |
| 용매 | Acetone | HCID 180 | — |
| 용매 | Water | HCID 962 | — |
| 생성물 | 6-(N-Chloroacetylaminomethyl)-5-hydroxy-4-sulfamoylindane | HCID 13210355 | — |
반응 단계
33.8 g (0.1 mole) of 6-(N-chloroacetylaminomethyl)-5-hydroxy-4-chlorosulfonylindane are dissolved in a little acetone, and the solution is added dropwise to 50 ml of concentrated ammonia solution. The mixture is stirred for 30 minutes at room temperature and is diluted with water. The precipitate which is deposited is filtered off with suction and dissolved in acetone, and the solution is filtered and stirred into water again.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04607030 |
| 출처 데이터셋 | uspto-grants-1986_08 |
| ORD ID | ord-014011e3e98841fd98e40d5753661173 |
| 출처 메모 | uspto-grants-1986_08 |