Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Acetophenone → Ethyl 2-(2-Butyl)-3-hydroxy-3-methyl-3-phenylpropionate
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Acetophenone | HCID 7410 | — |
| 반응물 | Ethyl 3-methylpentanoate | HCID 560255 | — |
| 생성물 | Ethyl 2-(2-Butyl)-3-hydroxy-3-methyl-3-phenylpropionate | HCID 13742288 | 36% |
반응 단계
The reaction of acetophenone (12 grams, 0.1 mole) with the enolate of ethyl 3-methylvalerate (14.4 grams, 0.1 mole) is carried out in the manner described in Example I. Distillation yields 9.5 grams (36%) of the pure product, b.p. 75°-80° C. (air bath temperature) at 0.05 mm Hg. I.R., N.M.R. and M.S. data confirm the above structure.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04607118 |
| 출처 데이터셋 | uspto-grants-1986_08 |
| ORD ID | ord-31bdf04c50534b1f8c9c6d14aa8d725e |
| 출처 메모 | uspto-grants-1986_08 |