Acetophenone → Ethyl 2-Isopropyl-3-hydroxy-3-methyl-3-phenylpropionate

반응식

[C:1]([C:4]1[CH:9]=[CH:8][CH:7]=[CH:6][CH:5]=1)(=[O:3])[CH3:2].[C:10]([O:16][CH2:17][CH3:18])(=[O:15])[CH2:11][CH:12]([CH3:14])[CH3:13]>>[CH:12]([CH:11]([C:1]([OH:3])([CH3:2])[C:4]1[CH:9]=[CH:8][CH:7]=[CH:6][CH:5]=1)[C:10]([O:16][CH2:17][CH3:18])=[O:15])([CH3:14])[CH3:13]

참가 물질

반응물 2

HCID 7410Acetophenone

HCID 7945Ethyl isovalerate

생성물 1

HCID 15575790Ethyl 2-Isopropyl-3-hydroxy-3-methyl-3-phenylpropionate

실험 절차

The material undergoes smooth pyrolysis when injected into a gas chromatography column (at about 230° C.) to generate acetophenone and ethyl isovalerate.

후처리

custominjected into a gas chromatography column (at about 230° C.)

출처 및 근거

ORD 기록: ord-1b498451e22e480c9e7be79ad02c51ff
출처 데이터셋: uspto-grants-1986_08
DOI: 10.6084/m9.figshare.5104873.v1
특허 번호: US04607118

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