참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|
| 반응물 | N-Methyloctadecylamine | HCID 75539 | — |
| 반응물 | Propanoic acid, 3-(diphenylphosphino)-, ethyl ester | HCID 280676 | — |
| 반응물 | Sodium Methoxide | HCID 10942334 | — |
| 생성물 | 3-(Diphenylphosphanyl)-N-methyl-N-octadecylpropanamide | HCID 53933128 | — |
반응 단계
A mixture of 5.7 g ethyl-3-diphenylphosphinopropionate (9.9 mmoles), 5.1 g N-methyl-n-octadecylamine (18.0 mmoles), and 0.3 g sodium methoxide (5.6 mmoles) were first deoxygenated and then heated to 100° C. under a nitrogen atmosphere for 24 hours. The mixture was then cooled and extracted with pentane. The pentane soluble was rotovapped to an oil.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 특허 번호 | US04608444 |
|---|
| 출처 데이터셋 | uspto-grants-1986_08 |
|---|
| ORD ID | ord-742f13ee5dcc41a9afa0a9d6004cf557 |
|---|
| 출처 메모 | uspto-grants-1986_08 |
|---|
