Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
1-(2-Methoxyphenyl)piperazine → 3-(4-(2-Methoxyphenyl)piperazin-1-yl)propanenitrile
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 1-(2-Methoxyphenyl)piperazine | HCID 1346 | — |
| 반응물 | Acrylonitrile | HCID 7855 | — |
| 용매 | Ethanol | HCID 702 | — |
| 생성물 | 3-(4-(2-Methoxyphenyl)piperazin-1-yl)propanenitrile | HCID 1822604 | 91.7% |
반응 단계
A solution of acrylonitrile (1.06 g, 20 mmol) in ethanol (50 ml) was added to a stirred solution of 2-methoxyphenylpiperazine (3.84 g, 20 mmol) in ethanol (100 ml). After 18 h, the solvent was evaporated in vacuo to give the product (4.5 g) as a white solid.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US06127357 |
| 출처 데이터셋 | uspto-grants-2000_10 |
| ORD ID | ord-22fea30183c04db69593e05118e5f118 |
| 출처 메모 | uspto-grants-2000_10 |