HCID 23291432, 화합물 → HCID 86755873, 화합물
반응식
[CH3:1][O:2][C:3]([C:5]1[CH:6]=[CH:7][CH:8]=[C:9]2[C:14]=1[S:13][CH2:12][CH:11]=[CH:10]2)=[O:4]>C(O)C>[CH3:1][O:2][C:3]([C:5]1[CH:6]=[CH:7][CH:8]=[C:9]2[C:14]=1[S:13][CH2:12][CH2:11][CH2:10]2)=[O:4]참가 물질
3
실험 절차
Methyl-2H-thiochromene-8-carboxylate (1.83 g, 8.88 mmol) was dissolved in ethanol (100 ml) and treated with 10% PdC (1.5 g). The mixture was then hydrogenated at atmospheric pressure at room temperature. After 19 h the reaction mixture was filtered through celite and evaporated under reduced pressure to give a colourless oil which was dried in vacuo to give the title compound (1.25 g, 68%)
후처리
- customwas then hydrogenated at atmospheric pressure at room temperature
- filtrationAfter 19 h the reaction mixture was filtered through celite
- customevaporated under reduced pressure
- customto give a colourless oil which
- customwas dried in vacuo
출처 및 근거
- ORD 기록
- ord-9680596c3be5453198746b0c0ed7cdcb
- 출처 데이터셋
- uspto-grants-2000_10
- 특허 번호
- US06127379
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