Hydrogen Peroxide → HCID 178444799, 화합물

HRID 36540

반응식

HRID 36540 반응식
[CH2:1]([CH:5]([CH2:9][NH:10][CH2:11][CH2:12][C:13]([OH:15])=[O:14])[C:6]([OH:8])=[O:7])[CH2:2][CH2:3][CH3:4].C(N(CC(O)=O)CC(O)=O)CN(CC(O)=O)CC(O)=[O:21].OO>O>[CH2:1]([CH:5]([CH2:9][NH:10][CH2:11][CH2:12][C:13]([OH:15])=[O:14])[C:6]([OH:8])=[O+:7][O-:21])[CH2:2][CH2:3][CH3:4]

참가 물질

5

반응물 3

HCID 784Hydrogen PeroxideHCID 6049Ethylenediaminetetraacetic AcidHCID 131718997Butyl imino dipropionic acid

생성물 1

HCID 178444799HCID 178444799, 화합물

시약·촉매·용매 1

HCID 962Water용매

반응 조건

온도
50 °C

실험 절차

100 g butyl imino dipropionic acid (0.46 mol) from example 7a was dissolved in 100 g H2O, whereupon 0.10 g EDTA was added and the temperature was increased to 50° C. After 30 minutes 3.2 g (0.475 mol) 50% hydrogen peroxide was added by drops during 20 minutes and the mixture reacted for 2 hours at 75° C. under a reflux cooler. Then the water was evaporated at 40° C. until a slightly yellow-brown oil formed.

후처리

  1. additionwas added
  2. customthe mixture reacted for 2 hours at 75° C. under a reflux cooler
  3. customThen the water was evaporated at 40° C. until a slightly yellow-brown oil
  4. customformed

출처 및 근거

ORD 기록
ord-21e0230d66d34335bfad3ff73829e671
출처 데이터셋
uspto-grants-1995_05
특허 번호
US05415668

연결된 노트

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