3-(p-Tolyl)acrylic acid → HCID 53411298, 화합물

HRID 36544

반응식

HRID 36544 반응식
[CH3:1][C:2]1[CH:12]=[CH:11][C:5]([CH:6]=[CH:7][C:8](O)=[O:9])=[CH:4][CH:3]=1.S(Cl)([Cl:15])=O>C1C=CC=CC=1>[CH3:1][C:2]1[CH:12]=[CH:11][C:5]([CH:6]=[CH:7][C:8]([Cl:15])=[O:9])=[CH:4][CH:3]=1

참가 물질

4

반응물 2

HCID 158353-(p-Tolyl)acrylic acidHCID 24386Thionyl Chloride

생성물 1

HCID 53411298HCID 53411298, 화합물

시약·촉매·용매 1

HCID 241Benzene용매

실험 절차

100 ml of benzene was added to 16.2 grams of p-methylcinnamic acid. 12 ml of thionyl chloride was added dropwise slowly thereto at ambient temperature. The temperature was elevated to 70° C. and the heating was continued until foaming ceased. Benzene and thionyl chloride were distilled off and the residue was dried thoroughly under reduced pressure.

후처리

  1. customat ambient temperature
  2. customwas elevated to 70° C.
  3. distillationBenzene and thionyl chloride were distilled off
  4. customthe residue was dried thoroughly under reduced pressure

출처 및 근거

ORD 기록
ord-d6ba12aed537467b89a9f21407689e48
출처 데이터셋
uspto-grants-1995_05
특허 번호
US05415780

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