Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Thionyl Chloride → 3-(3-Pyridyl)acryloyl chloride hydrochloride
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Thionyl Chloride | HCID 24386 | — |
| 반응물 | 3-(3-Pyridinyl)-2-propenoic acid | HCID 101984 | — |
| 용매 | Benzene | HCID 241 | — |
| 생성물 | 3-(3-Pyridyl)acryloyl chloride hydrochloride | HCID 71360027 | — |
반응 단계
67 ml of benzene was added to 10 grams of 3-(3-pyridyl)-acrylic acid. 8.1 ml of thionyl chloride was added dropwise slowly thereto at ambient temperature. The temperature was elevated to 70° C. and the heating was continued until foaming ceased. Benzene and thionyl chloride were distilled off and the residue was dried thoroughly under reduced pressure.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US05415780 |
| 출처 데이터셋 | uspto-grants-1995_05 |
| ORD ID | ord-c47a2810ac0e4dcd8f71084b2669a25f |
| 출처 메모 | uspto-grants-1995_05 |