Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Water → (2,6-Dimethyl-3-nitrophenyl)methanol
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Water | HCID 962 | — |
| 반응물 | Sodium Hydroxide | HCID 14798 | — |
| 반응물 | (2,6-Dimethyl-3-nitrophenyl)methyl acetate | HCID 10537042 | — |
| 용매 | Methanol | HCID 887 | — |
| 생성물 | (2,6-Dimethyl-3-nitrophenyl)methanol | HCID 10487641 | 82.4% |
반응 단계
To a solution of 2,6-dimethyl-3-nitrobenzyl acetate (26.9 g) in methanol (266 ml) was added aqueous 1N sodium hydroxide solution (133 ml) at ambient temperature for 30 minutes. To the mixture was added water, and the precipitate was collected by filtration to give 2,6-dimethyl-3-nitrobenzyl alcohol (18.0 g) as pale yellow crystals.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US06127389 |
| 출처 데이터셋 | uspto-grants-2000_10 |
| ORD ID | ord-f1fb1725b3bb469d9f57f73a62124038 |
| 출처 메모 | uspto-grants-2000_10 |