Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
(S)-1-(3-Chlorophenyl)ethane-1,2-diol → (s)-(2-(3-Chlorophenyl)-2-hydroxyethyl)oxocarboxamide
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | (S)-1-(3-Chlorophenyl)ethane-1,2-diol | HCID 10130180 | — |
| 반응물 | (s)-(2-(3-Chlorophenyl)-2-carbamoyloxyethyl)oxocarboxamide | HCID 131721943 | — |
| 용매 | Methanol | HCID 887 | — |
| 생성물 | (s)-(2-(3-Chlorophenyl)-2-hydroxyethyl)oxocarboxamide | HCID 131721942 | 25% |
반응 단계
(S)-(2-(3-Chlorophenyl)-2-carbamoyloxyethyl)oxocarboxamide (1.36 g, yield 25%, m.p. 117-119° C., [α]D =12.88 (c=2.30, MeOH) was prepared using the same synthetic method described in Example 20, except (S)-1-m-chlorophenyl-1,2-ethanediol was used instead of (DL)-1-m-chlorophenyl-1,2-ethanediol.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US06127412 |
| 출처 데이터셋 | uspto-grants-2000_10 |
| ORD ID | ord-6cfca9cd125a4350a3f7dbb8723965ae |
| 출처 메모 | uspto-grants-2000_10 |