Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Bromoacetyl chloride → 4-Bromoacetyl-7-methoxy-2,3,4,5-tetrahydro-1,4-benzothiazepine
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Bromoacetyl chloride | HCID 89602 | — |
| 반응물 | 7-Methoxy-2,3,4,5-tetrahydro-1,4-benzothiazepine | HCID 11805628 | — |
| 용매 | Triethylamine | HCID 8471 | — |
| 생성물 | 4-Bromoacetyl-7-methoxy-2,3,4,5-tetrahydro-1,4-benzothiazepine | HCID 15291645 | 51.5% |
반응 단계
7-Methoxy-2,3,4,5-tetrahydro-1,4-benzothiazepine (3.0 g), triethylamine (3.1 g) and bromoacetyl chloride (3.2 g) were reacted in the same manner as in Experimental Example 1 to give 4-bromoacetyl-7-methoxy-2,3,4,5-tetrahydro-1,4-benzothiazepine (2.5 g).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US05416066 |
| 출처 데이터셋 | uspto-grants-1995_05 |
| ORD ID | ord-f2d9bc7a547848ad9da613d6416d1ac8 |
| 출처 메모 | uspto-grants-1995_05 |