참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|
| 반응물 | 1,2-Bis(chloromethyl)benzene | HCID 11919 | — |
| 반응물 | Phthalimide potassium salt | HCID 24194345 | — |
| 생성물 | HCID 57925620 | HCID 57925620 | — |
반응 단계
A mixture of α,α'-dichloroxylene (8.75 g, 50 mmol) and potassium phthalimide (5.6 g, 30 mmol) was heated to 50° C. for 24 h. Then the reaction mixture was concentrated in vacuo, dissolved in ethyl acetate and, after usual work-up, the desired compound was obtained by flash chromatography on silica gel (ethyl acetate:hexane; 15:85) (6 g, 65%).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 특허 번호 | US05416076 |
|---|
| 출처 데이터셋 | uspto-grants-1995_05 |
|---|
| ORD ID | ord-83c234a702b148d187820f5614fe44cc |
|---|
| 출처 메모 | uspto-grants-1995_05 |
|---|
