참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|
| 반응물 | 3-Chloro-2-chloromethyl-1-propene | HCID 15859 | — |
| 반응물 | Phthalimide potassium salt | HCID 24194345 | — |
| 용매 | Dimethylformamide | HCID 6228 | — |
| 생성물 | HCID 19937309 | HCID 19937309 | — |
반응 단계
A mixture of 3-chloro-2-chloromethyl-1-propene (6.55 g, 50 mmol) and potassium phthalimide (5.6 g, 30 mmol) in anhydrous dimethylformamide (200 ml) was heated two days at 50° C. Then the mixture was concentrated in vacuo and, after usual work-up, the product was purified by flash chromatography on silica gel (ethyl acetate:hexane; 15:85) (4.2 g, 78%).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 특허 번호 | US05416076 |
|---|
| 출처 데이터셋 | uspto-grants-1995_05 |
|---|
| ORD ID | ord-abdb5a943ca24c13acd5d001c7bd8c59 |
|---|
| 출처 메모 | uspto-grants-1995_05 |
|---|
