Cyclopentadiene → HCID 23289326, 화합물

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[CH:1]1[CH:6]=[C:5](/[CH:7]=[CH:8]/[N+:9]([O-])=O)[C:4]([Cl:12])=[CH:3][CH:2]=1.[CH:13]1[CH2:17][CH:16]=[CH:15][CH:14]=1>>[Cl:12][C:4]1[CH:3]=[CH:2][CH:1]=[CH:6][C:5]=1[CH:7]1[CH:15]2[CH2:16][CH:17]([CH:13]=[CH:14]2)[CH:8]1[NH2:9]

참가 물질

반응물 2

HCID 7612Cyclopentadiene

HCID 5369313(E)-1-Chloro-2-(2-nitrovinyl)benzene

생성물 1

HCID 23289326HCID 23289326, 화합물

실험 절차

This material (LC-MS m/z 220 (MH+)) was prepared via the nitro derivative according to the procedure described in Preparation 92 but starting instead with 2-chloro-omega-nitrostyrene and cyclopentadiene.

후처리

customdescribed in Preparation 92

출처 및 근거

ORD 기록: ord-1c93fee8a5a14e35940e12fe42671935
출처 데이터셋: uspto-grants-2000_10
DOI: 10.6084/m9.figshare.5104873.v1
특허 번호: US06130217

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