Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
N-(2-methylprop-2-enyl)-N-(2,2-dimethoxyethyl)-urethane → N-(2-Methylprop-2-enyl)-N-(2-oxoethyl)-urethane
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | N-(2-methylprop-2-enyl)-N-(2,2-dimethoxyethyl)-urethane | HCID 15069986 | — |
| 용매 | Acetone | HCID 180 | — |
| 용매 | Water | HCID 962 | — |
| 생성물 | N-(2-Methylprop-2-enyl)-N-(2-oxoethyl)-urethane | HCID 15069992 | — |
반응 단계
11.5 g (50 mmol) of N-(2-methylprop-2-enyl)-N-(2,2-dimethoxyethyl)-urethane and 1.25 g (5 mmol) of pyridinium p-toluenesulphate in 100 ml of acetone and 10 ml of water are heated under reflux for two days. The mixture is concentrated and the residue is distilled.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US05416096 |
| 출처 데이터셋 | uspto-grants-1995_05 |
| ORD ID | ord-fe5669ce784443e29808812c8f8571c0 |
| 출처 메모 | uspto-grants-1995_05 |