Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
L-Valine → 2-[2-[2-(1-Carboxy-2-methylpropylcarbamoyl) phenyldisulfanyl]benzoylamino]-3-methylbutanoic acid
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | L-Valine | HCID 6287 | — |
| 반응물 | 2,2'-Dithiodibenzoyl chloride | HCID 88164 | — |
| 생성물 | 2-[2-[2-(1-Carboxy-2-methylpropylcarbamoyl) phenyldisulfanyl]benzoylamino]-3-methylbutanoic acid | HCID 465364 | — |
반응 단계
Using the method employed in Preparation 30, 17.8 g (0.15 mol) of D,L valine was reacted with 17.2 g (0.05 mol) of 2,2'-dithiobisbenzoyl chloride to produce 11.4 g of the title compound after recrystallization from acetic acid, mp 226.5-227.5° C.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US06133270 |
| 출처 데이터셋 | uspto-grants-2000_10 |
| ORD ID | ord-c59ad78ae3394bdbbe3c7de766e63148 |
| 출처 메모 | uspto-grants-2000_10 |