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Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
HRID 36731생성일: 2026년 10월 23일

2,6-Di-t-butyl-p-benzoquinone → 2,6-Di-tertiary-butyl-4-(4'-cyanomethylphenylimino)-2,5-cyclohexadiene-1-one

https://huagongshe.com/ko/reaction/36731

반응식

참여 물질

역할이름HCID투입량
반응물2,6-Di-t-butyl-p-benzoquinoneHCID 12867—
반응물4-AminophenylacetonitrileHCID 77000—
생성물2,6-Di-tertiary-butyl-4-(4'-cyanomethylphenylimino)-2,5-cyclohexadiene-1-oneHCID 22401559—

반응 단계

Using the method of Example 1, 4-aminobenzylcyanide was reacted with 2,6-di-tertiary-butyl-p-benzoquinone to give 2,6-di-tertiary-butyl-4-(4'-cyanomethylphenylimino)-2,5-cyclohexadiene-1-one, m.p. 126.5°-127.5° C. Following the reduction method of Example 1, Step B, the corresponding anilino phenylacetonitrile, m.p. 146°-147° C., was obtained. This was converted to 5-[4-(3,5-di-t-butyl-4-hydroxyanilino)benzyl]tetrazole, m.p. 212°-214° C. (dec), following the method of Example 30, but carried out at 110° C. for 48 hours.

출처 및 근거

DOI10.6084/m9.figshare.5104873.v1
특허 번호US05416113
출처 데이터셋uspto-grants-1995_05
ORD IDord-0667c16ef61a44ee8420eb89fd26b0da
출처 메모uspto-grants-1995_05