Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Silane, chloro(chloromethyl)dimethyl- → n,n-Diethyl-2-chloro-6-[(chloromethyl)dimethylsilyl]benzamide
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Silane, chloro(chloromethyl)dimethyl- | HCID 74393 | — |
| 반응물 | 2-Chloro-N,N-diethylbenzamide | HCID 82566 | — |
| 생성물 | n,n-Diethyl-2-chloro-6-[(chloromethyl)dimethylsilyl]benzamide | HCID 18630016 | — |
반응 단계
The title compound was prepared according to General Method A from the compound of Example e and 1.5 eq (chloromethyl)dimethylsilyl chloride. Purification by HPLC using 1:9 ethyl acetate/hexanes gave 5.4 g of the desired compound as a yellow oil, an 85% yield.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US06133252 |
| 출처 데이터셋 | uspto-grants-2000_10 |
| ORD ID | ord-50db707cf0e149059d1bd51e3d57c7ab |
| 출처 메모 | uspto-grants-2000_10 |