Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Silane, chloro(chloromethyl)dimethyl- → n-Ethyl-2-chloro-6-[(chloromethyl)dimethylsilyl]benzamide
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Silane, chloro(chloromethyl)dimethyl- | HCID 74393 | — |
| 반응물 | 2-chloro-N-ethylbenzamide | HCID 347962 | — |
| 생성물 | n-Ethyl-2-chloro-6-[(chloromethyl)dimethylsilyl]benzamide | HCID 18630074 | — |
반응 단계
The title compound was prepared from the compound of Example f and 2.0 eq (chloromethyl)dimethylsilyl chloride according to General Method C. Recrystallization from ethyl acetate gave 3.0 g of the desired compound as a white solid, a 52% yield. m.p. 88-89° C.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US06133252 |
| 출처 데이터셋 | uspto-grants-2000_10 |
| ORD ID | ord-5559485b8ba34a3ba66d94109c8a8114 |
| 출처 메모 | uspto-grants-2000_10 |