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Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
HRID 368823생성일: 2026년 10월 26일

6-Chloro-1-(2-chloroethyl)isochroman → 1-[2-(6-Chloroisochroman-1-yl)ethyl]-4-(4-methoxyphenyl)piperazine dihydrochloride

https://huagongshe.com/reaction/368823

반응식

참여 물질

역할이름HCID투입량
반응물6-Chloro-1-(2-chloroethyl)isochromanHCID 23288787—
반응물1-[2-(Isochroman-1-yl)ethyl]-4-(2-methoxyphenyl)piperazine dihydrochloride monohydrateHCID 23288951—
생성물1-[2-(6-Chloroisochroman-1-yl)ethyl]-4-(4-methoxyphenyl)piperazine dihydrochlorideHCID 23288911—

반응 단계

Following the general procedure of EXAMPLE 1 and making non-critical variations but using 6-chloro-1-(2-chloroethyl)isochroman (LXIV, 0.2315 g, 0.972 mmol) and 1-(4-methoxyphenyl)piperazine dihydrochloride (XI, 0.3772 g, 1.00 mmol), the title compound is obtained, mp 203.5-208°; MS (m/z) 386; IR (mineral oil) 1512, 2388, 1485, 1261, 1118 and 1105 cm-1.

출처 및 근거

DOI10.6084/m9.figshare.5104873.v1
특허 번호US06133446
출처 데이터셋uspto-grants-2000_10
ORD IDord-8c87741abd554547b76b1a96b369cb96
출처 메모uspto-grants-2000_10