참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|
| 반응물 | N-vinyl-2-pyrrolidone | HCID 6917 | — |
| 반응물 | Triphenyltin Chloride | HCID 12540 | — |
| 용매 | O-Xylene | HCID 7237 | — |
| 생성물 | N-vinylpyrrolidone triphenyltin chloride | HCID 86740183 | — |
반응 단계
The same reactor as used in Example 1 was charged with 30 g of N-vinylpyrrolidone, 104 g of triphenyltin chloride and 200 g of xylene, and the mixture was stirred at 50° C. for 2 hours to form an N-vinylpyrrolidone/triphenyltin chloride adduct. Then, 50 g of butyl acrylate, 16 g of octyl acrylate and 0.5 g of benzoyl peroxide were added, and with stirring, the mixture was heated to 75° C. At this temperature, 0.2 g of benzoyl peroxide was added three times at intervals of 3 hours, and the polymerization reaction was carried out for a total of 12 hours to give an N-coordinated-triphenyltin-containing copolymer solution having a molecular weight of 77,000 (to be referred to as a copolymer solution [A-18]). This copolymer solution was used directly as an antifouling agent.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 특허 번호 | US04526932 |
|---|
| 출처 데이터셋 | uspto-grants-1985_07 |
|---|
| ORD ID | ord-8a58580ccd064a9c91bd6696538e305f |
|---|
| 출처 메모 | uspto-grants-1985_07 |
|---|