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Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
HRID 370515생성일: 2026년 10월 25일

N-vinyl-2-pyrrolidone → N-vinylpyrrolidone triphenyltin chloride

https://huagongshe.com/reaction/370515

반응식

참여 물질

역할이름HCID투입량
반응물N-vinyl-2-pyrrolidoneHCID 6917—
반응물Triphenyltin ChlorideHCID 12540—
용매O-XyleneHCID 7237—
생성물N-vinylpyrrolidone triphenyltin chlorideHCID 86740183—

반응 조건

온도50 °C

반응 단계

The same reactor as used in Example 1 was charged with 30 g of N-vinylpyrrolidone, 104 g of triphenyltin chloride and 200 g of xylene, and the mixture was stirred at 50° C. for 2 hours to form an N-vinylpyrrolidone/triphenyltin chloride adduct. Then, 50 g of butyl acrylate, 16 g of octyl acrylate and 0.5 g of benzoyl peroxide were added, and with stirring, the mixture was heated to 75° C. At this temperature, 0.2 g of benzoyl peroxide was added three times at intervals of 3 hours, and the polymerization reaction was carried out for a total of 12 hours to give an N-coordinated-triphenyltin-containing copolymer solution having a molecular weight of 77,000 (to be referred to as a copolymer solution [A-18]). This copolymer solution was used directly as an antifouling agent.

출처 및 근거

DOI10.6084/m9.figshare.5104873.v1
특허 번호US04526932
출처 데이터셋uspto-grants-1985_07
ORD IDord-8a58580ccd064a9c91bd6696538e305f
출처 메모uspto-grants-1985_07