Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Indole-3-Acetic Acid → HCID 12219383, 화합물
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Indole-3-Acetic Acid | HCID 802 | — |
| 반응물 | Oxalyl chloride | HCID 65578 | — |
| 용매 | Dimethylformamide | HCID 6228 | — |
| 용매 | Dichloromethane | HCID 6344 | — |
| 생성물 | HCID 12219383 | HCID 12219383 | — |
반응 단계
To indole-3-acetic acid (186 mg, 1.06 mmol) in 3.5 mL of methylene chloride and 0.009 mL of dimethylformamide, oxalyl chloride (2 M in methylene chloride, 0.64 mL, 1.27 mmol) was added. The mixture was stirred at room temperature for 1 hour and concentrated to give 1H-indole-3-acetyl chloride.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US05420123 |
| 출처 데이터셋 | uspto-grants-1995_05 |
| ORD ID | ord-b5bb6f04c7054cc0b42ddca249e133b1 |
| 출처 메모 | uspto-grants-1995_05 |