Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
3-Bromoaniline → 2,2'-Dithiobis[N-(3-bromophenyl)benzamide]
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 3-Bromoaniline | HCID 11562 | — |
| 반응물 | 2,2'-Dithiodibenzoyl chloride | HCID 88164 | — |
| 용매 | Pyridine | HCID 1049 | — |
| 용매 | Dichloromethane | HCID 6344 | — |
| 생성물 | 2,2'-Dithiobis[N-(3-bromophenyl)benzamide] | HCID 18935308 | 55.8% |
반응 단계
This compound was prepared according to the general method of Example 77 using 2,2'-dithiobisbenzoyl chloride (2.00 g, 5.83 mmol) in 50 mL of dichloromethane and 3-bromoaniline (1.98 g, 11.6 mmol) in 16 mL of pyridine. The crude product was recrystallized from ethyl acetate-hexanes to yield 1.99 g of the title compound, mp 194°-196° C.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US05734081 |
| 출처 데이터셋 | uspto-grants-1998_03 |
| ORD ID | ord-b72f28adf1044fce8dbba03ec99cbcd2 |
| 출처 메모 | uspto-grants-1998_03 |