Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Trifluoroacetyl chloride → 1-hydroxy-5,6-dichloro-2-trifluoromethyl-1H-imidazo(4,5-b)-pyridine
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Trifluoroacetyl chloride | HCID 61106 | — |
| 반응물 | 5,6-Dichloro-3-nitropyridin-2-amine | HCID 15392047 | — |
| 반응물 | 5,6-Dichloro-2-trifluoroacetamido-3-nitropyridine | HCID 20355477 | — |
| 생성물 | 1-hydroxy-5,6-dichloro-2-trifluoromethyl-1H-imidazo(4,5-b)-pyridine | HCID 20355499 | — |
반응 단계
In like procedures, 5,6-dichloro-2-amino-3-nitropyridine was reacted with trifluoroacetyl chloride and the resulting 5,6-dichloro-2-trifluoroacetamido-3-nitropyridine was hydrogenated to obtain 1-hydroxy-5,6-dichloro-2-trifluoromethyl-1H-imidazo(4,5-b)-pyridine, m.p. 207°-208° C.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04087432 |
| 출처 데이터셋 | uspto-grants-1978_05 |
| ORD ID | ord-a0c16f6717aa49e3969304dbb3913955 |
| 출처 메모 | uspto-grants-1978_05 |