Acetic Acid → 2-nitroethyl Acetate

HRID 371677

반응식

HRID 371677 반응식
[N+:1]([CH:4](O)[CH3:5])([O-:3])=[O:2].[C:7]([OH:10])(=[O:9])[CH3:8].C1C=CC=CC=1>OS(O)(=O)=O.O>[N+:1]([CH2:4][CH2:5][O:10][C:7](=[O:9])[CH3:8])([O-:3])=[O:2]

참가 물질

6

반응물 3

HCID 176Acetic AcidHCID 241BenzeneHCID 22056827HCID 22056827, 화합물

생성물 1

HCID 118153992-nitroethyl Acetate

시약·촉매·용매 2

HCID 1118Sulfuric Acid촉매HCID 962Water용매

실험 절차

64 g nitroethanol, 50 ml glacial acetic acid, 250 ml benzene and 5 drops conc. H2SO4 were refluxed, using a water separator for 8 hours; 12 ml of H2O were collected. The solution was evaporated and vacuum distilled (1 mm at 60° C) yielding 89 g colorless nitroethylacetate.

후처리

  1. customfor 8 hours
  2. custom12 ml of H2O were collected
  3. customThe solution was evaporated
  4. distillationvacuum distilled (1 mm at 60° C)

출처 및 근거

ORD 기록
ord-87691613a2f4415f94d673a2b49d15d6
출처 데이터셋
uspto-grants-1978_05
특허 번호
US04087438

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