Diethylamine → HCID 18756985, 화합물

HRID 371702

반응식

HRID 371702 반응식
[CH2:1]([NH:3][CH2:4][CH3:5])[CH3:2].[C:6]([CH2:9][P:10](=[O:15])([O:13]C)[O:11]C)(O)=[O:7].C1(N=C=NC2CCCCC2)CCCCC1>C(Cl)Cl>[CH2:1]([N:3]([CH2:4][CH3:5])[C:6]([CH2:9][P:10](=[O:15])([OH:13])[OH:11])=[O:7])[CH3:2]

참가 물질

5

반응물 3

HCID 8021DiethylamineHCID 10868DicyclohexylcarbodiimideHCID 1899642-(Dimethoxyphosphoryl)acetic acid

생성물 1

HCID 18756985HCID 18756985, 화합물

시약·촉매·용매 1

HCID 6344Dichloromethane용매

실험 절차

Diethylamine (0.045 mole) and dimethyl (carboxymethyl)phosphonate (0.04 mole) were dissolved in 100 ml. of methylene chloride. As the solution was stirred, dicyclohexylcarbodiimide was added portionwise. The solution was stirred overnight and the mixture was filtered. The filtrate was concentrated to a solid. It was recrystallized from an appropriate solvent such as methanol.

후처리

  1. stirringThe solution was stirred overnight
  2. filtrationthe mixture was filtered
  3. concentrationThe filtrate was concentrated to a solid
  4. customIt was recrystallized from an appropriate solvent such as methanol

출처 및 근거

ORD 기록
ord-9643680f67894807ab01548cbca04a9a
출처 데이터셋
uspto-grants-1978_05
특허 번호
US04087522

연결된 노트

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