Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Hydrochloric Acid → Hydrochloric Acid
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Hydrochloric Acid | HCID 313 | — |
| 반응물 | Ethanol | HCID 702 | — |
| 반응물 | Gabapentin | HCID 3446 | — |
| 생성물 | Hydrochloric Acid | HCID 313 | — |
| 생성물 | Ethyl 2-[1-(aminomethyl)cyclohexyl]acetate | HCID 15512485 | — |
반응 단계
10 g. of the 1-aminomethyl-1-cyclohexane-acetic acid, prepared according to Example 1, are dissolved in 50 ml. anhydrous ethanol and saturated at 0° C. with gaseous hydrogen chloride. The reaction mixture is left to stand overnight at ambient temperature, then evaporated in a vacuum and the residue recrystallised from ethanol/ether. Ethyl 1-aminomethyl-1-cyclohexane-acetate is obtained in the form of its hydrochloride; m.p. 161° - 163° C.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04087544 |
| 출처 데이터셋 | uspto-grants-1978_05 |
| ORD ID | ord-405a81cc00a14ab4b6003f57296c8be8 |
| 출처 메모 | uspto-grants-1978_05 |