Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
6-Methoxyquinoline → Quinoline, 1,2,3,4-tetrahydro-6-methoxy-
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 6-Methoxyquinoline | HCID 14860 | — |
| 촉매 | Palladium | HCID 23938 | — |
| 용매 | Ethanol | HCID 702 | — |
| 생성물 | Quinoline, 1,2,3,4-tetrahydro-6-methoxy- | HCID 67113 | 94.6% |
반응 단계
6-Methoxyquinoline (1.00g) was dissolved in absolute ethanol (20 ml) and hydrogenated under pressure in the presence of 10% palladium on charcoal (0.10g) with shaking for about 40 hours. Filtration and evaporation to dryness of the filtrate gave 1,2,3,4-tetrahydro-6-methoxyquinoline as a light-brown gum (0.97g). The structure was supported by nmr spectrum.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04087561 |
| 출처 데이터셋 | uspto-grants-1978_05 |
| ORD ID | ord-1d27416b936e4f4b9c7fc294a512a2d7 |
| 출처 메모 | uspto-grants-1978_05 |