Acrylonitrile → 3-(Dioctadecylamino)propionitrile

HRID 371783

반응식

HRID 371783 반응식
[CH2:1]([NH:19][CH2:20][CH2:21][CH2:22][CH2:23][CH2:24][CH2:25][CH2:26][CH2:27][CH2:28][CH2:29][CH2:30][CH2:31][CH2:32][CH2:33][CH2:34][CH2:35][CH2:36][CH3:37])[CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH2:10][CH2:11][CH2:12][CH2:13][CH2:14][CH2:15][CH2:16][CH2:17][CH3:18].[C:38](#[N:41])[CH:39]=[CH2:40]>>[CH2:20]([N:19]([CH2:1][CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH2:10][CH2:11][CH2:12][CH2:13][CH2:14][CH2:15][CH2:16][CH2:17][CH3:18])[CH2:40][CH2:39][C:38]#[N:41])[CH2:21][CH2:22][CH2:23][CH2:24][CH2:25][CH2:26][CH2:27][CH2:28][CH2:29][CH2:30][CH2:31][CH2:32][CH2:33][CH2:34][CH2:35][CH2:36][CH3:37]

참가 물질

3

반응물 2

HCID 7855AcrylonitrileHCID 66989Dioctadecylamine

생성물 1

HCID 223391003-(Dioctadecylamino)propionitrile

실험 절차

3-(Dioctadecylamino)propionitrile is prepared by refluxing a mixture of dioctadecylamine (200 g.) and acrylonitrile (1903.8 ml.) for eighteen hours. The mixture is then concentrated to a waxy semi-solid which is slurried in acetone, filtered, and air dried overnight.

후처리

  1. temperatureby refluxing
  2. concentrationThe mixture is then concentrated to a waxy semi-solid which
  3. filtrationfiltered
  4. customair dried overnight

출처 및 근거

ORD 기록
ord-4e784c4e26e14199b4fb1e5dd57e98b0
출처 데이터셋
uspto-grants-1978_05
특허 번호
US04087552

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