Bromine → 2-Amino-3-bromo-N,N-diethyl-5-methoxy-benzylamine

HRID 371874노트

반응식

HRID 371874 반응식
[NH2:1][C:2]1[CH:13]=[CH:12][C:11]([O:14][CH3:15])=[CH:10][C:3]=1[CH2:4][N:5]([CH2:8][CH3:9])[CH2:6][CH3:7].[Br:16]Br>C(Cl)Cl>[NH2:1][C:2]1[C:13]([Br:16])=[CH:12][C:11]([O:14][CH3:15])=[CH:10][C:3]=1[CH2:4][N:5]([CH2:8][CH3:9])[CH2:6][CH3:7]

참가 물질

4

반응물 2

HCID 24408BromineHCID 4220092-Amino-N,N-diethyl-5-methoxy-benzylamine

생성물 1

HCID 203192402-Amino-3-bromo-N,N-diethyl-5-methoxy-benzylamine

시약·촉매·용매 1

HCID 6344Dichloromethane용매

실험 절차

2-Amino-3-bromo-N,N-diethyl-5-methoxy-benzylamine was prepared from 2-amino-N,N-diethyl-5-methoxy-benzylamine and bromine analogous to Example 9. Proof of structure by IR-, UV- and NMR-spectra. IR-spectrum (methylenechloride): 3250 cm-1NH2 ; 3410 cm-1NH2 ; 2830 cm-1OCH3 ; 2800 cm-1N-ethyl; 1480 cm-1C=C; 1590 cm-1C=C.

출처 및 근거

ORD 기록
ord-20fe7e2ac203496bb8d96aa7643e52f9
출처 데이터셋
uspto-grants-1978_05
특허 번호
USRE029628

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