Methyl Acrylate → Methyl 2-hexadecylaminopropionate

HRID 371894

반응식

HRID 371894 반응식
[CH2:1]([NH2:17])[CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH2:10][CH2:11][CH2:12][CH2:13][CH2:14][CH2:15][CH3:16].[C:18]([O:22][CH3:23])(=[O:21])[CH:19]=[CH2:20]>CO>[CH2:1]([NH:17][CH:19]([CH3:20])[C:18]([O:22][CH3:23])=[O:21])[CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH2:10][CH2:11][CH2:12][CH2:13][CH2:14][CH2:15][CH3:16]

참가 물질

4

반응물 2

HCID 7294Methyl AcrylateHCID 8926Hexadecylamine

생성물 1

HCID 15919806Methyl 2-hexadecylaminopropionate

시약·촉매·용매 1

HCID 887Methanol용매

실험 절차

66.4 g of hexadecylamine are dissolved in 250 ml of methanol. 27 ml of methyl acrylate are added and the mixture is left to stand overnight. After removal of the solvent by distillation the residue is recrystallised from ethyl acetate.

후처리

  1. waitthe mixture is left
  2. customAfter removal of the solvent
  3. distillationby distillation the residue
  4. customis recrystallised from ethyl acetate

출처 및 근거

ORD 기록
ord-7c99f89006944ecc9fb1dc936a498189
출처 데이터셋
uspto-grants-1978_05
특허 번호
US04088491

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