Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
1-Hexyne → 1-(4-Bromophenyl) 2-heptyn-1-one
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 1-Hexyne | HCID 12732 | — |
| 반응물 | 4-Bromobenzoyl chloride | HCID 68515 | — |
| 용매 | Triethylamine | HCID 8471 | — |
| 생성물 | 1-(4-Bromophenyl) 2-heptyn-1-one | HCID 54449136 | — |
반응 단계
The following were stirred at ambient temperature for about 2 hours 30 minutes, 49 ml of 1-hexyne, 75 ml of triethylamine, 40 mg of cuprous iodide, 40 mg of bis triphenylphosphine palladium dichloride and 9 g of parabromobenzoyl chloride.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US05420138 |
| 출처 데이터셋 | uspto-grants-1995_05 |
| ORD ID | ord-63ea4cacfe084abf827121e185cfa069 |
| 출처 메모 | uspto-grants-1995_05 |