Butylamine → HCID 178449232, 화합물

HRID 372223

반응식

HRID 372223 반응식
CS/[C:3](/[NH2:6])=[N:4]/[NH2:5].[IH:7].[NH2:8][CH2:9][CH2:10][CH2:11][CH3:12]>O>[IH:7].[NH2:5][NH:4][C:3]([NH:8][CH2:9][CH2:10][CH2:11][CH3:12])=[NH:6]

참가 물질

4

반응물 2

HCID 8007ButylamineHCID 6508896Methyl hydrazinecarbimidothioate hydroiodide

생성물 1

HCID 178449232HCID 178449232, 화합물

시약·촉매·용매 1

HCID 962Water용매

실험 절차

S-Methylisothiosemicarbazide hydroiodide (46.6 g) and 1-aminobutane (48 ml) and water (100 ml) were heated under reflux for 1 hour. The resulting solution was evaporated to an oil which was crystallised from amyl alcohol/80-100 PE, to give the title compound (a).

후처리

  1. temperatureunder reflux for 1 hour
  2. customThe resulting solution was evaporated to an oil which
  3. customwas crystallised from amyl alcohol/80-100 PE

출처 및 근거

ORD 기록
ord-f2bacff0b3604575b7f45e3420a48d67
출처 데이터셋
uspto-grants-1978_05
특허 번호
US04089962

연결된 노트

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