Ammonium Hydroxide → Urea, (1,2,3,4-tetrahydro-4-oxo-1-naphthalenyl)-

HRID 372276노트

반응식

HRID 372276 반응식
[O:1]=[C:2]1[C:11]2[C:6](=[CH:7][CH:8]=[CH:9][CH:10]=2)[CH:5]([N:12]=[C:13]=[O:14])[CH2:4][CH2:3]1.[OH-].[NH4+:16]>O1CCCC1>[O:1]=[C:2]1[C:11]2[C:6](=[CH:7][CH:8]=[CH:9][CH:10]=2)[CH:5]([NH:12][C:13]([NH2:16])=[O:14])[CH2:4][CH2:3]1

참가 물질

4

반응물 2

HCID 14923Ammonium HydroxideHCID 203516844-Isocyanato-3,4-dihydronaphthalen-1(2H)-one

생성물 1

HCID 3628438Urea, (1,2,3,4-tetrahydro-4-oxo-1-naphthalenyl)-

시약·촉매·용매 1

HCID 8028Tetrahydrofuran용매

실험 절차

1,2,3,4-Tetrahydro-4-oxo-1-naphthylisocyanate (5.0 g) in tetrahydrofuran is added to a rapidly stirred aqueous concentrated ammonium hydroxide solution (excess) to afford 1,2,3,4-tetrahydro-4-oxo-1-naphthylurea.

출처 및 근거

ORD 기록
ord-9354fdd672124ccda68defaffe0471eb
출처 데이터셋
uspto-grants-1978_05
특허 번호
US04089976

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