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4-amino-3,4-dihydro-2H-naphthalen-1-one → Urea, (1,2,3,4-tetrahydro-4-oxo-1-naphthalenyl)-

HRID 372278
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인쇄 미리보기

반응식

HRID 372278 반응식
[O:1]=[C:2]1[C:11]2[C:6](=[CH:7][CH:8]=[CH:9][CH:10]=2)[CH:5]([NH2:12])[CH2:4][CH2:3]1.C([NH:15][C:16](=O)[O-:17])C>C(O)C>[O:1]=[C:2]1[C:11]2[C:6](=[CH:7][CH:8]=[CH:9][CH:10]=2)[CH:5]([NH:12][C:16]([NH2:15])=[O:17])[CH2:4][CH2:3]1
참가 물질실험 절차후처리출처 및 근거반응 노트

참가 물질

4

반응물 2

HCID 137386604-amino-3,4-dihydro-2H-naphthalen-1-oneHCID 22042200N-ethylcarbamate

생성물 1

HCID 3628438Urea, (1,2,3,4-tetrahydro-4-oxo-1-naphthalenyl)-

시약·촉매·용매 1

HCID 702Ethanol용매

실험 절차

Equimolar quantities of 1,2,3,4-tetrahydro-4-oxo-1-naphthylamine and ethylcarbamate are mixed and heated until ethanol is no longer released. The crude product, 1,2,3,4-tetrahydro-4-oxo-1-naphthylurea is washed with water then with cold ethanol and dried.

후처리

  1. washThe crude product, 1,2,3,4-tetrahydro-4-oxo-1-naphthylurea is washed with water
  2. dry with materialwith cold ethanol and dried

출처 및 근거

ORD 기록
ord-36ba6e2674064fc0b1a3e0ce6fb0ba8c
출처 데이터셋
uspto-grants-1978_05
DOI
10.6084/m9.figshare.5104873.v1
특허 번호
US04089976

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