HCID 12803422, 화합물 → 1-(2-Methoxyethyl)-4-phenylimidazolidin-2-one
반응식
[CH3:1][O:2][CH2:3][CH2:4][N:5]1[CH:9]=[C:8]([C:10]2[CH:15]=[CH:14][CH:13]=[CH:12][CH:11]=2)[NH:7][C:6]1=[O:16].[H][H]>[Pd].C(O)C>[CH3:1][O:2][CH2:3][CH2:4][N:5]1[CH2:9][CH:8]([C:10]2[CH:15]=[CH:14][CH:13]=[CH:12][CH:11]=2)[NH:7][C:6]1=[O:16]참가 물질
5
실험 절차
Approximately 10.9 g. of 1-(2-methoxyethyl)-4-phenyl-4-imidazolin-2-one and 1 g. of 10% palladium on carbon in 100 ml. of ethanol is hydrogenated in a Parr Shaker apparatus at 30 psig of hydrogen for 45 minutes. The catalyst is filtered, washed with ethanol, and the filtrate is concentrated to give the title compound as a waxy white solid; m.p. 82°-83° C.
후처리
- filtrationThe catalyst is filtered
- washwashed with ethanol
- concentrationthe filtrate is concentrated
출처 및 근거
- ORD 기록
- ord-c27e73e5cf334303a7a897592f6e5fe3
- 출처 데이터셋
- uspto-grants-1978_05
- 특허 번호
- US04090025
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