HCID 12803438, 화합물 → HCID 13093657, 화합물
반응식
[CH3:1][O:2][CH2:3][CH2:4][N:5]1[CH:9]=[C:8]([C:10]2[CH:15]=[CH:14][CH:13]=[CH:12][CH:11]=2)[N:7]([C:16](=[O:18])[CH3:17])[C:6]1=[O:19].[H][H]>[Pd].C(O)C>[CH3:1][O:2][CH2:3][CH2:4][N:5]1[CH2:9][CH:8]([C:10]2[CH:11]=[CH:12][CH:13]=[CH:14][CH:15]=2)[N:7]([C:16](=[O:18])[CH3:17])[C:6]1=[O:19]참가 물질
5
실험 절차
Approximately 3.9 g. of 1-(2-methoxyethyl)-3-acetyl-4-phenyl-4-imidazolin-2-one and 400 mg. of 10% palladium on carbon in 30 ml. of ethanol is hydrogenated in the Parr Shaker apparatus at 30 psig of hydrogen. After one hour the catalyst is filtered and washed with 50 ml. of ethanol. The combined filtrate is concentrated to yield the title compounds as a colorless oil.
후처리
- filtrationAfter one hour the catalyst is filtered
- washwashed with 50 ml
- concentrationThe combined filtrate is concentrated
출처 및 근거
- ORD 기록
- ord-a6814553d39e4a479f4c5ef37a8e10ed
- 출처 데이터셋
- uspto-grants-1978_05
- 특허 번호
- US04090025
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