Methylcarbamyl fluoride → N-Methyl-N(Phenylthiosulfenyl)Carbamoyl Fluoride

HRID 372372노트

반응식

HRID 372372 반응식
[C:1]1([S:7][S:8]Cl)[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=1.[CH3:10][NH:11][C:12]([F:14])=[O:13]>>[CH3:10][N:11]([S:8][S:7][C:1]1[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=1)[C:12]([F:14])=[O:13]

참가 물질

3

반응물 2

HCID 12545956Methylcarbamyl fluorideHCID 15683250Phenylthiosulfenyl chloride

생성물 1

HCID 23332999N-Methyl-N(Phenylthiosulfenyl)Carbamoyl Fluoride

실험 절차

Prepared by the procedure of Example II by reacting phenylthiosulfenyl chloride with methylcarbamoyl fluoride. b.p. 100°-110° C/0.3 Torr ND22.5 1.5770.

후처리

  1. customPrepared by the procedure of Example II

출처 및 근거

ORD 기록
ord-a948376d85b24205a633fefe4353694e
출처 데이터셋
uspto-grants-1978_05
특허 번호
US04091016

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