1H-Indole-3-thiol → 3-(Indol-3-ylthio)crotonic acid

HRID 372756노트

반응식

HRID 372756 반응식
[SH:1][C:2]1[C:10]2[C:5](=[CH:6][CH:7]=[CH:8][CH:9]=2)[NH:4][CH:3]=1.[C:11]([OH:16])(=[O:15])[C:12]#[C:13][CH3:14]>>[NH:4]1[C:5]2[C:10](=[CH:9][CH:8]=[CH:7][CH:6]=2)[C:2]([S:1]/[C:13](/[CH3:14])=[CH:12]\[C:11]([OH:16])=[O:15])=[CH:3]1

참가 물질

3

실험 절차

-- By the same method as described in Example 1, 0.2 mole each of 3-mercaptoindole and tetrolic acid gives 10.2 g of product after recrystallization from acetonitrile, mp 201°-202° C.

출처 및 근거

ORD 기록
ord-e63ef72f637e4bdb844b98e7cba99425
출처 데이터셋
uspto-grants-1978_05
특허 번호
US04092328

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