Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Hydrochloric Acid → Ethyl phosphonoacetate
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Hydrochloric Acid | HCID 313 | — |
| 반응물 | Phosphonoacetic Acid | HCID 546 | — |
| 반응물 | Ethanol | HCID 702 | — |
| 생성물 | Ethyl phosphonoacetate | HCID 3614325 | — |
반응 단계
Into 100 ml. of absolute ethanol was placed 28 g. (0.2 mole) of phosphonoacetic acid. The solution was treated with a stream of dry hydrogen chloride at 0° C. for 45 minutes. After refluxing for 3 hours the solution was allowed to stand overnight at room temperature. Evaporation of the solvent yielded a viscous oil, which was dried in vacuo over P2O5 and NaOH.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04092412 |
| 출처 데이터셋 | uspto-grants-1978_05 |
| ORD ID | ord-5ffe54c0372844fe9942268a808f2423 |
| 출처 메모 | uspto-grants-1978_05 |